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Ibiglustat-L-Malic-acid-LCMS-37227-MedChemExpress

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MS Report from Instrument: LCMS-03 File ..MS03\\Data\\20190130\\20190130\\MXY15-002-1.D Tgt Mass (CHM): Injection Date : 30 Jan 19 10:31 am +0800 Seq. Line : 25 Sample Name : MXY15-002-1 Location : P1-C-01 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20190130\\20190130\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20190130\\20190130\\1-POS-3MIN.M Catalog No : HY-16743A Batch#37227 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-392 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1.3531.2561.3171.386mAU200000.5 DAD1 B, Sig=2,4 Ref=offmAU50000.5 ELS1 A, ELSD SignalmV111000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701000000500000000.51 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.70.050-0.05-0.100.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off1.522.5min1.3791.466111.2561.3171.3531.3842.0142.1491.522.5min2.0151.522.5min1.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.26 0.02 0.60 0.57 0.14 102 1.32 0.02 0.92 0.82 0.21 390 1.35 0.02 430.77 476.71 98.07 390 1.39 0.01 5.93 10.02 1.35 390 2.01 0.01 0.47 0.52 0.11 336 2.15 0.02 0.56 0.57 0.13 114 Integration Results for DAD1 B, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.26 0.01 0.13 0.13 0.11 102 1.32 0.01 0.21 0.24 0.17 390 1.35 0.02 121.13 134.53 98.40 390 1.38 0.01 1.46 2.53 1.19 390 2.02 0.01 0.16 0.19 0.13 336 Integration Results for ELS1 A, ELSD SignalLCMS-03 1/31/2019 11:21:12 AM SYSTEMPage1 of4MS Report from Instrument: LCMS-03|-------|--------|--------------|--------------|--------|------| 1.47 0.07 9.65 2.18 100.00 390 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.38 0.06 4229190.00 1087315.00 100.00 390 RetTim Width Area Height Area% MS(+)LCMS-03 1/31/2019 11:21:12 AM SYSTEMPage2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.38 <<<< POSITIVE SPECTRA >>>> ES-API Positive7000060000500004000030000102.2195.6392.120000100000100200300400500600700800900m/z390.2LCMS-03 1/31/2019 11:21:12 AM SYSTEMPage3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 1/31/2019 11:21:12 AM SYSTEMPage4 of4

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